McDermott Group

John

David Muñoz-Panaigua, Ph.D.

Contact Information
NINT 1-117
National Institute for Nanotechnology
National Research Council Canada
11421 Saskatchewan Drive
Edmonton, Alberta, T6G 2M9

Phone: 780 641-1711
Fax: 780 641-1601
E-mail: david.munoz-paniagua@nrc-cnrc.gc.ca

Group Members

Employment:
- Research Associate, Sensors and Devices, National Institute for Nanotechnology, National Research Council of Canada, Edmonton, Alberta. 2006-2012.
- Postdoctoral Fellow, Department of Chemistry, The University of Western Ontario, London, Ontario. 2005-2006.

Education
- Ph.D. Physical Chemistry, The University of Western Ontario, London, Ontario. 2005. "Development of Interfacial Force Microscopy:Applications for Materials and Interfaces".
- B.Sc. Chemical Sciences, Monterrey Institute of Technology and Superior Studies, Monterrey, Nuevo Leon. Mexico. 1998. "Synthesis and Characterisation of a Ruthenium Photo-Sensitiser for Low-Cost Solar Panels".

Research:

  • Interested in the study of material properties of technologically relevant materials heterogeneous on a sub-micrometre length-scale and errors tracking in nanoindentation experiments.
  • Building a new generation environmentally controlled Interfacial Force Microscope (IFM). The construction of this IFM incorporates several important new instrumental features:
    • Environmental chamber ~1-105 Pa range with humidity meter and software controlled bleed-in valves
    • Encoded sample positioning stage with accuracy of 20nm/1.4mm per axis
    • Isolated ground feed-throughs
    • Heating/cooling sample stage ~200 to 600 K in vacuo ~255 to 375 K in dry N2 with instability <10 mK.
    • A closed-loop scanning stage with 30x30x10μm scan envelope and sub-nanometer precision.
  • Studying nano-indentation calibration methodologies and the error they introduce into data analysis; proposed a new mathematical model that helps minimise said error.
  • Development of a facile low-cost sapphire indentation tip fabrication process. Planning, design and implementation of a processing station for sapphire indentation tip
  • Developing a novel tunnelling-junction micro-fabrication technique in collaboration with Wayne Hiebert (Principal Investigator at NRC-NINT).
  • Design and implementation of a dip-coater with an embedded micro-controller for asphaltene sample preparation by a COSI sponsored post-doctoral fellow in the Department of Chemistry at the University of Alberta.
  • Advising a graduate student in the Department of Pharmacology on experimental design and interpretation of data obtained from bone cross-sections of test rats.
  • Directing a graduate student in the Department of Mechanical Engineering at the University of Alberta in the design of a new MEMS based IFM sensor.
  • Consulting for the Integrated Nano-Systems Research Facility at the University of Alberta with regards to their SPM and nano-indentation services.

Recent Publications:
- D. J. Munoz-Paniagua, R. Lister, K. Cao "A Novel Procedure for the Preparation of Out-of-Plane Tunnelling Junctions for MEMS Transduction and Sensing" National Research Council Canada Report of Invention, in preparation.
- Y. Wu, S.M. Adeeb, M. J. Duke, D. Munoz-Paniagua, M. R. Doschak "Compositional and Material Properties of Rat Bone after Bisphosphonate and/or Strontium Ranelate Drug Treatment", Journal of Bone & Mineral Research, submitted April 2011.
- D. J. Munoz-Paniagua, M. T. McDermott, P. R. Norton, S. Tadayyon, "Direct Tip Shape Determination of a Berkovich Indenter: Effect on Nanomechanical Property Measurement and Description of a Worn Indenter", IEEE Transactions on Nanotechnology, 9(4), 487, 2010.
- D. J. Munoz-Paniagua, K. Cao "A Method to Produce Sapphire Needles of Controlled Geometry of a Crystalline Monofilament" National Research Council Canada Report of Invention, 12266-0, 15-03-2010.
- J.E. Decker, A. Bogdanov, B.J. Eves, D. Goodchild, L. Johnston, N. Kim, M. McDermott, D. Munoz-Paniagua, J.R. Pekelsky, S. Wingar, and S. Zou, "Developments in Metrology in Support of Nanotechnology," in Proceedings of the 3rd International Symposium on Nanotechnology in Construction, Z. Bittnar, P. J. M. Bartos, J. Nemecek, V. Smilauer, and J. Zeman, Eds. Berlin, Heidelberg: Springer Berlin Heidelberg, pp. 71-80, 2009.
- S. Ruffell, J. E. Bradby, J. S. Williams, D. Munoz-Paniagua, S. Tadayyon, L. L. Coatsworth and P. R. Norton, "Nanoindentation-induced phase transformations in silicon at elevated temperatures", Nanotechnology 20(13), 135603, 2009.
- D. Shakhvorostov, M. H. Müser, N. J. Mosey, D. Munoz-Paniagua, G. Pereira, Y. Song, M. Kasrai, P. R. Norton, "On the pressure-induced loss of crystallinity in orthophosphates of zinc and calcium", Journal of Chemical Physics, 128(7),074706, 2008.
- G. Pereira, A. Lachenwitzer, D. Munoz-Paniagua, M. Kasrai, P. R. Norton, T. W. Capehart, T. A. Perry, Y. T. Cheng, "Nanoscale chemistry and mechanical properties of tribofilms on an Al-Si alloy (A383) Interaction of ZDDP, calcium detergent and a molybdenum friction modifier" Tribology Materials, Surfaces & Interfaces, 1(1), pp.4-17, 2007.
- G. Pereira, D. Munoz-Paniagua, A. Lachenwitzer, M. Kasrai, P. R. Norton, T. W. Capehart, T. A. Perry, Y.-T. Cheng "A variable temperature mechanical analysis of ZDDP antiwear films formed on 52100 steel" Wear, 262, pp. 461-470, 2007.
- G. Pereira, A. Lachenwitzer, D. Munoz-Paniagua, M. Kasrai, P. R. Norton, M. Abrecht and P.U.P.A. Gilbert, "The role of the cation in antiwear films formed from ZDDP on 52100 steel", Tribology Letters, 23(2), pp. 109-119, 2006.
- C. Zhang, J. Luo, D. Munoz-Paniagua, P. R. Norton, "The hydroxylation of passive oxide films on X-70 steel by dissolved hydrogen studied by nuclear reaction analysis, Auger electron spectroscopy, X-ray photoelectron spectroscopy and secondary ion mass spectroscopy", Thin Solid Films, 503, pp. 149 - 157, 2006.