Isolation of biphenyl

Recall that in the "Separation" of the mixture you removed 2-bromobenzoic acid* by converting it to its corresponding water-soluble salt*.

Biphenyl* (a neutral compound*) remained dissolved in the dichloromethane* (CH2Cl2) solution. Neutral compounds do not undergo salt formation.

The dichloromethane solution should be washed with water to remove water-soluble inorganic impurities, then dried, and the excess dichloromethane removed.

What will you do to remove the solvent (CH2Cl2) from biphenyl?

Back extraction
Filtration
Distillation

Organic Web Chem University of Alberta